Inficon HAPSITE ER Chemical Identification System Manuel d'utilisateur

OPERATING MANUALHAPSITE® ERChemical Identification SystemIPN 074-471-P1B

CE Implementation Date: October 2004 Authorized Representative: Duane H. Wright Operations Quality Manager, ISS INFICON Inc.

3 - 16 IPN 074-471-P1B HAPSITE ER Operating Manual3.2.1 Changing the Default MethodThe default method for the HAPSITE ER can be changed. By changing

3 - 17IPN 074-471-P1BHAPSITE ER Operating Manual3.2.2 Show AllThe HAPSITE will only show methods that are compatible with the current sample and/or

3 - 18 IPN 074-471-P1B HAPSITE ER Operating Manual2 When powered on or taken out of Extended Standby, the HAPSITE will automatically start preparing

3 - 19IPN 074-471-P1BHAPSITE ER Operating Manual5 Using the touch screen, touch RUN SURVEY. See Figure 3-32.Figure 3-32 Survey Ready6 Alternately,

3 - 20 IPN 074-471-P1B HAPSITE ER Operating Manual8 Sample air away from the point of concern for one minute. Remember to note the background TIC. Se

3 - 21IPN 074-471-P1BHAPSITE ER Operating Manual10 By touching CMPD ID, a list of identified compounds will appear. See Figure 3-37. The CAS number,

3 - 22 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 3-39 Sample GRAPH function13 When the TIC begins to increase, move the probe away from the

3 - 23IPN 074-471-P1BHAPSITE ER Operating Manual15 If an Analyze method is not going to be run, touch STOP to stop the sampling process and automati

3 - 24 IPN 074-471-P1B HAPSITE ER Operating Manual3.3.1 Quick Reference SOP — Survey Method1 If you are running an Analyze (GC/MS) method after Surv

3 - 25IPN 074-471-P1BHAPSITE ER Operating Manual3.4 ANALYZE (GC/MS) Mode with the Concentrator3.4.1 The Tri- Bed ConcentratorThe Tri-Bed concentra

WARRANTY AND LIABILITY - LIMITATION: Seller warrants the products manufactured by it, or by an affiliated company and sold by it, and described on the

3 - 26 IPN 074-471-P1B HAPSITE ER Operating Manual4 Using the touch screen, touch RUN ANALYZE. See Figure 3-43.Figure 3-43 Analyze Button5 Alternate

3 - 27IPN 074-471-P1BHAPSITE ER Operating ManualFigure 3-45 Collecting Sample For Concentrator RunCAUTIONDo not touch the sample with the probe. Do

3 - 28 IPN 074-471-P1B HAPSITE ER Operating Manual8 By touching CMPD ID, a list of found compounds will appear. See Figure 3-47. This page will displ

3 - 29IPN 074-471-P1BHAPSITE ER Operating ManualFigure 3-48 Sample Chromatogram View For Concentrator10 A METHOD FINISHED message will appear when

3 - 30 IPN 074-471-P1B HAPSITE ER Operating Manual3.4.4 Quick Reference SOP —Concentrator Methods1 Verify that the concentrator is installed.2 Refer

3 - 31IPN 074-471-P1BHAPSITE ER Operating Manual3.5 Detecting Hazardous ChemicalsIf the HAPSITE Analyze message turns red, a chemical’s concentrati

3 - 32 IPN 074-471-P1B HAPSITE ER Operating Manual3.5.1 View Results/View ReportsData files and reports can be viewed from the main front panel scre

3 - 33IPN 074-471-P1BHAPSITE ER Operating ManualFigure 3-53 Arrow Keys4 To view files from another method, use the SELECT RESULTS button. See Figur

3 - 34 IPN 074-471-P1B HAPSITE ER Operating Manual6 The big blue arrows are used to scroll through the peaks in the chromatogram. The identified comp

3 - 35IPN 074-471-P1BHAPSITE ER Operating Manual8 Touching a specific compound on the screen will display that compound’s synonym and exposure limit

3 - 36 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 3-60 CLOSE 11 Touching the CMPD ID (Compound Identification) button while in Review Results

3 - 37IPN 074-471-P1BHAPSITE ER Operating Manual12 Touching a specific compound in the list will display that compound’s synonym and exposure limits

3 - 38 IPN 074-471-P1B HAPSITE ER Operating Manual14 To view the Summary, Qualitative and Quantitative Reports, touch the REPORTS button. Alternately

3 - 39IPN 074-471-P1BHAPSITE ER Operating Manual16 The Qualitative Report can be found be touching the QUAL key. See Figure 3-66. Alternately, highl

3 - 40 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 3-68 Type of Method

3 - 41IPN 074-471-P1BHAPSITE ER Operating Manual3.6 The Help IconThe Help icon is located on the upper right of the front panel. See Figure 3-69. F

3 - 42 IPN 074-471-P1B HAPSITE ER Operating Manual3.7 The Info IconThe Info icon is located next to the Help icon in the right hand corner of the up

3 - 43IPN 074-471-P1BHAPSITE ER Operating Manual1 An important resource on this database is The NIOSH Pocket Guide to Chemical Hazards (NPG). See Fi

3 - 44 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 3-74 NIOSH Pocket Guide

3 - 45IPN 074-471-P1BHAPSITE ER Operating Manual3 Scroll down to display an alphabet. Touch the first letter of the desired compound. See Figure 3-7

IPN 074-471-P1BHAPSITE ER Operating ManualDefinition ofNote, Hint, Danger, Warning and Caution ParagraphsNOTE: This is a note paragraph. Notes provid

3 - 46 IPN 074-471-P1B HAPSITE ER Operating Manual5 Touch the desired chemical. The Pocket Guide for that specific chemical will be displayed. See Fi

3 - 47IPN 074-471-P1BHAPSITE ER Operating Manual7 To access information regarding Immediately Dangerous to Life or Health Concentrations (IDLHs), to

3 - 48 IPN 074-471-P1B HAPSITE ER Operating Manual9 Scroll down, press DOWN or use the down arrow key to find the desired compound. Press the link to

3 - 49IPN 074-471-P1BHAPSITE ER Operating Manual3.7.1 HAPSITE IconThe HAPSITE icon provides information about the System Parameters and the operati

3 - 50 IPN 074-471-P1B HAPSITE ER Operating Manual3.7.1.1 Battery IconIf a battery is installed, the Battery icon will display information about the

3 - 51IPN 074-471-P1BHAPSITE ER Operating Manual3.7.1.3 Internal Standard IconThe Internal Standard icon uses a vertical bar graph correlate the an

3 - 52 IPN 074-471-P1B HAPSITE ER Operating Manual3.7.1.4.1 HEATERS IconTouching the HEATERS icon provides the current temperatures of the column, t

3 - 53IPN 074-471-P1BHAPSITE ER Operating Manual3.7.1.4.3 CONC ButtonInformation about the concentrator can be found through this button. After tou

3 - 54 IPN 074-471-P1B HAPSITE ER Operating Manual3.7.1.5 TUNE STATUS IconThis icon provides information about the state of the HAPSITE’s tune. If t

3 - 55IPN 074-471-P1BHAPSITE ER Operating Manual3.7.1.5.1 TUNE REPORTSWhen the TUNE STATUS icon has been touched, see Figure 3-93, a button, TUNE R

IPN 074-471-P1B HAPSITE ER Operating ManualOperating Manual Style ConventionsThe following information describes the conventions used throughout this

3 - 56 IPN 074-471-P1B HAPSITE ER Operating Manual3.7.1.6 GPS IconThe GPS icon will provide the latitude and longitude coordinates of the HAPSITE’s

3 - 57IPN 074-471-P1BHAPSITE ER Operating Manual3.7.1.7.1 HAPS ButtonThe HAPS button will provide the HAPSITE name, the HAPSITE’s Serial Number, an

3 - 58 IPN 074-471-P1B HAPSITE ER Operating Manual3.7.1.7.3 DATE TIME ButtonThis button displays the present date and time. See Figure 3-99.Figure 3

3 - 59IPN 074-471-P1BHAPSITE ER Operating ManualThe SKIP HEATER option allows for the HAPSITE to run when the probe is cold. This is useful in cold

3 - 60 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 3-102 Exit Menu2 The three exit options will be displayed on the screen. There will also be

3 - 61IPN 074-471-P1BHAPSITE ER Operating ManualFigure 3-104 Confirming Shutdown4 For Turn Off, the screen will become dark and the HAPSITE will tu

3 - 62 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 3-105 Extended Standby2 When the screen prompts, Do you want to go into Standby?, touch Yes

3 - 63IPN 074-471-P1BHAPSITE ER Operating Manual4 When the screen prompts, Do you want to go into Standby?, touch Yes. Alternately, using the arrow

3 - 64 IPN 074-471-P1B HAPSITE ER Operating Manual3.8.1.1 End Standby1 To End Standby, touch END STANDBY or using the arrow keys, highlight END STAN

3 - 65IPN 074-471-P1BHAPSITE ER Operating Manual3.9 Analyze (GC/MS) Mode with Headspace Sampling System in Portable ModeThe Headspace Sampling Syst

TOC - 1IPN 074-471-P1BHAPSITE ER Operating ManualTable Of ContentsTrademarksDefinition of Note, Hint, Danger, Warning and Caution ParagraphsOperatin

3 - 66 IPN 074-471-P1B HAPSITE ER Operating Manual5 When powered on or taken out of Extended Standby, the HAPSITE will automatically start preparing

3 - 67IPN 074-471-P1BHAPSITE ER Operating Manual9 Gently push the Headspace needle into the 40 mL vial containing the blank/sample. 10 The screen wi

3 - 68 IPN 074-471-P1B HAPSITE ER Operating Manual12a The CMPD ID screen can also be accessed by using the arrow keys to highlight CMPD ID and pushin

3 - 69IPN 074-471-P1BHAPSITE ER Operating Manual14 At the end of the Headspace run, a prompt will appear. When prompted Insert needle into a clean v

3 - 70 IPN 074-471-P1B HAPSITE ER Operating Manual3.9.1 Quick Reference SOP — GC/MS Mode with HSS in Portable Mode1 Verify that the desired sampling

3 - 71IPN 074-471-P1BHAPSITE ER Operating Manual3.10 SituProbeFor complete information on SituProbe methods, see Chapter 14, SituProbe. For instruc

3 - 72 IPN 074-471-P1B HAPSITE ER Operating Manual8 Using the touch screen, touch RUN ANALYZE. If using the push buttons, push ANALYZE RUN.Figure 3-1

3 - 73IPN 074-471-P1BHAPSITE ER Operating Manual10 The next screen will prompt Sampling is Done. See Figure 3-123. Again, no action is required by t

3 - 74 IPN 074-471-P1B HAPSITE ER Operating Manual12 To view the chromatogram while the method is running, touch GRAPH. Alternately, use the arrow ke

3 - 75IPN 074-471-P1BHAPSITE ER Operating Manual3.10.2 Quick Reference SOP — GC/MS Mode with SituProbe in Portable Mode1 Verify that the desired sa

TOC - 2 IPN 074-471-P1B HAPSITE ER Operating Manual2.3 Helpful Guidelines . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

3 - 76 IPN 074-471-P1B HAPSITE ER Operating ManualThis page is intentionally blank.

4 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 4Wireless and Touch Screen Options4.1 Wireless Option4.1.1 IntroductionThe HAPSITE has a wi

4 - 2 IPN 074-471-P1B HAPSITE ER Operating ManualCAUTIONTo maintain compliance with FCC standards and regulations and to ensure the proper operation

4 - 3IPN 074-471-P1BHAPSITE ER Operating Manual4.1.3 Regulatory Compliance Information for CANADIAN UsersThis section of the Operating Manual lists

4 - 4 IPN 074-471-P1B HAPSITE ER Operating Manual4.1.4 Regulatory Compliance Information for EUROPEAN UsersThis section of the Operating Manual list

4 - 5IPN 074-471-P1BHAPSITE ER Operating ManualThis symbol indicates that usage restrictions apply to this equipment. Such marking indicates that th

4 - 6 IPN 074-471-P1B HAPSITE ER Operating Manual4.1.4.3 European Safety Compliance StatementThis device has been tested and certified according to

4 - 7IPN 074-471-P1BHAPSITE ER Operating Manual4.1.5 Wireless RangeThe HAPSITE is equipped with an 802.11b/g wireless adapter. The typical range fo

4 - 8 IPN 074-471-P1B HAPSITE ER Operating ManualDANGERThe HAPSITE contains a wireless transmitter/receiver that emits electromagnetic radiation (EMR

4 - 9IPN 074-471-P1BHAPSITE ER Operating Manual4.1.7.1 Setting the User Access LevelThe HAPSITE leaves the factory in Normal operating mode. Settin

TOC - 3IPN 074-471-P1BHAPSITE ER Operating ManualChapter 3Operating HAPSITE in Portable Mode3.1 Starting the HAPSITE in Portable Mode. . . . . . . .

4 - 10 IPN 074-471-P1B HAPSITE ER Operating Manual4.1.8 Wireless Module Indicator LightsLocated on the Wireless Module inside the HAPSITE front cove

4 - 11IPN 074-471-P1BHAPSITE ER Operating Manual1 Open the front panel of the HAPSITE.2 Remove the cover from the power switch (for the wireless rad

4 - 12 IPN 074-471-P1B HAPSITE ER Operating Manual4.2 The MAIN MenuThe MAIN menu contains the following options: View Results, Smart Interface, Adju

4 - 13IPN 074-471-P1BHAPSITE ER Operating Manual2 Alternately, use the arrow keys to highlight MAIN and push OK SEL. See Figure 4-7.Figure 4-7 Arro

4 - 14 IPN 074-471-P1B HAPSITE ER Operating Manual5 To exit the Smart Interface, touch CLOSE. See Figure 4-10.Figure 4-10 Smart Interface4.2.2 Adju

4 - 15IPN 074-471-P1BHAPSITE ER Operating Manual2 Touch Adjust Brightness. See Figure 4-12.Figure 4-12 Adjust Brightness3 A scroll bar will appear

4 - 16 IPN 074-471-P1B HAPSITE ER Operating Manual5 To completely darken the screen, touch Black Screen.Figure 4-15 Black Screen6 To exit the Black

4 - 17IPN 074-471-P1BHAPSITE ER Operating Manual4.3 Touch Screen OptionsNOTE: If the Touch Screen freezes, pushing the MENU and ESC keys at the sam

4 - 18 IPN 074-471-P1B HAPSITE ER Operating Manual3 Touch Calibrate or push OK SEL when Calibrate is highlighted. See Figure 4-19.Figure 4-19 Calibr

4 - 19IPN 074-471-P1BHAPSITE ER Operating Manual5 Instructions on screen calibration will appear. Touch OK or highlight OK and push OK SEL. See Figu

TOC - 4 IPN 074-471-P1B HAPSITE ER Operating Manual3.7.2 Attachments . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

4 - 20 IPN 074-471-P1B HAPSITE ER Operating Manual7 Touch OK in the next ten seconds if the calibration was accurate for all four targets. Otherwise,

4 - 21IPN 074-471-P1BHAPSITE ER Operating Manual2 From the drop-down menu, touch Touch Screen. Alternately, use the arrow keys to highlight Touch Sc

4 - 22 IPN 074-471-P1B HAPSITE ER Operating Manual4.3.2.2 Enabling the Touch Screen1 Using the arrow keys, highlight MAIN and touch OK SEL. See Figu

4 - 23IPN 074-471-P1BHAPSITE ER Operating Manual4.4 The USB Drive4.4.1 Copying Files to the USBData files can be saved to the USB drive on the HAP

4 - 24 IPN 074-471-P1B HAPSITE ER Operating Manual4 Touch the USB icon.Touch Copy to USB or using the arrow keys, highlight Copy to USB and push OK S

4 - 25IPN 074-471-P1BHAPSITE ER Operating Manual6 Touch the desired file for copying and touch Select. Alternately, use the arrow keys to highlight

4 - 26 IPN 074-471-P1B HAPSITE ER Operating Manual8 A bar will be displayed on the screen to show the download’s progress. Touch Close to return to t

4 - 27IPN 074-471-P1BHAPSITE ER Operating Manual4.4.2 Copying Files From the USBThe Copying Files from the USB button can be used to transfer metho

4 - 28 IPN 074-471-P1B HAPSITE ER Operating Manual4 Touch the USB icon. Touch COPY FROM USB or using the arrow keys, highlight COPY FROM USB and push

4 - 29IPN 074-471-P1BHAPSITE ER Operating Manual6 A progress bar will be shown on the screen. Touch Close to return to the USB screen. If another do

TOC - 5IPN 074-471-P1BHAPSITE ER Operating Manual4.4 The USB Drive . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

4 - 30 IPN 074-471-P1B HAPSITE ER Operating Manual4.4.3 Updating the Front Panel Software from the USBPeriodically, there may be updates to front pa

4 - 31IPN 074-471-P1BHAPSITE ER Operating Manual5 Touch the desired update and touch Select. See Figure 4-43NOTE: If there is not an update file on

4 - 32 IPN 074-471-P1B HAPSITE ER Operating Manual7 The following screen will be displayed while the system is updating. Touch Done to exit this scre

4 - 33IPN 074-471-P1BHAPSITE ER Operating Manual4.4.4 Retrieving Files from the USBOnce files have been save to the USB drive, they can be transfer

4 - 34 IPN 074-471-P1B HAPSITE ER Operating ManualThis page is intentionally blank.

5 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 5Operating HAPSITE in Laptop Mode5.1 Starting the HAPSITE in Laptop ModeStarting the HAPSITE

5 - 2 IPN 074-471-P1B HAPSITE ER Operating Manual5.2 Survey ModeThe Survey Mode is used for quick analysis and tentative results. The run period is

5 - 3IPN 074-471-P1BHAPSITE ER Operating Manual3 As part of the HAPSITE’s preparation, it will run AutoTune. If AutoTune successfully runs and compl

5 - 4 IPN 074-471-P1B HAPSITE ER Operating Manual8 Monitor the Probe distance indicator bar on the HAPSITE screen for guidance. See Figure 5-5. The b

5 - 5IPN 074-471-P1BHAPSITE ER Operating ManualFigure 5-7 Survey Run Complete11 To view the data, note the Data File name and click on the Data Rev

TOC - 6 IPN 074-471-P1B HAPSITE ER Operating Manual7.5 Manual Tune Settings and Controls. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 - 6 IPN 074-471-P1B HAPSITE ER Operating Manual5.2.1 Quick Reference SOP — Running Survey Mode1 Double-click the ER IQ software icon.2 Double-clic

5 - 7IPN 074-471-P1BHAPSITE ER Operating Manual5.3 Selecting a New Method1 Click the Abort button. See Figure 5-9.Figure 5-9 Aborting Method2 Doub

5 - 8 IPN 074-471-P1B HAPSITE ER Operating Manual3 Choose a folder that matches the physical configuration of the HAPSITE. In this example, the Conce

5 - 9IPN 074-471-P1BHAPSITE ER Operating Manual4 Click the desired method and then, click OK. This example shows the ER_Air_Tri-Bed_PPB_Standard.mth

5 - 10 IPN 074-471-P1B HAPSITE ER Operating Manual5.4 Analyze (GC/MS) Mode with Concentrator5.4.1 The Tri- Bed ConcentratorThis method is used for

5 - 11IPN 074-471-P1BHAPSITE ER Operating Manual5 A Concentrator Cleanout will also be run as part of the HAPSITE’s preparation. Hold the probe in a

5 - 12 IPN 074-471-P1B HAPSITE ER Operating Manual9 When prompted Sampling is Done on the HAPSITE screen, remove the probe from the sample source. Se

5 - 13IPN 074-471-P1BHAPSITE ER Operating ManualFigure 5-19 Concentrator Run Finished12 Review results at the end of the run. If red lines appear o

5 - 14 IPN 074-471-P1B HAPSITE ER Operating Manual5.4.3 Quick Reference SOP — Tri-Bed Concentrator Method1 Verify that the Concentrator is installed

5 - 15IPN 074-471-P1BHAPSITE ER Operating Manual5.5 Analyze (GC/MS) Mode with Headspace Sampling System The Headspace Sampling System is used to te

TOC - 7IPN 074-471-P1BHAPSITE ER Operating Manual8.9 ER IQ Controls . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

5 - 16 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 5-20 Headspace Needle6 When the HAPSITE has been turned on (refer to section Chapter 3 on p

5 - 17IPN 074-471-P1BHAPSITE ER Operating Manual10 Click RUN button on the pop-up window or from the Control Panel on the screen. Figure 5-22 Run B

5 - 18 IPN 074-471-P1B HAPSITE ER Operating Manual15 A METHOD FINISHED prompt will appear on the HAPSITE screen when the run is complete. See Figure

5 - 19IPN 074-471-P1BHAPSITE ER Operating Manual5.5.1 Quick Reference SOP — GC/MS Mode with HSS 1 Double-click the ER IQ software icon.2 Verify tha

5 - 20 IPN 074-471-P1B HAPSITE ER Operating Manual5.6 SituProbe MethodsRefer to the SituProbe Purge and Trap System Operating Manual for more inform

5 - 21IPN 074-471-P1BHAPSITE ER Operating Manual7 The screen will prompt Collecting Sample Now For. The SituProbe is automatically collecting a samp

5 - 22 IPN 074-471-P1B HAPSITE ER Operating Manual10 See Figure 5-31 for an example of a completed chromatogram from the Laptop.Figure 5-31 SituProb

5 - 23IPN 074-471-P1BHAPSITE ER Operating Manual5.6.2 Quick Reference SOP — Analyze Mode with SituProbe1 Double-click the ER IQ software icon.2 Ver

5 - 24 IPN 074-471-P1B HAPSITE ER Operating Manual5.7 Front Panel EmulatorThe HAPSITE ER can be operated using the front panel emulator. This option

6 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 6Methods6.1 Introduction to MethodsThe versatility of the HAPSITE lies in the variety of met

TOC - 8 IPN 074-471-P1B HAPSITE ER Operating Manual9.8.5 How to Grab Spectra/Utilize the Full NIST Program . . . . . . . . . . . . . . . . . 9-339.8

6 - 2 IPN 074-471-P1B HAPSITE ER Operating ManualCAUTIONAll unknown samples should first be collected with the Survey Method to estimate the total VO

6 - 3IPN 074-471-P1BHAPSITE ER Operating Manual6.1.3 Building a Survey Method Library FileSurvey methods can be designed for data collection in thr

6 - 4 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 6-2 Data File Information PageDuring the Calibration run, enter the concentration level of t

6 - 5IPN 074-471-P1BHAPSITE ER Operating ManualThe spectrum of the analyte must be recorded to the Target Compound Library. The spectrum is recorded

6 - 6 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 6-5 Grab Spectrum for Template WindowThe compound is displayed in the Analytes in Library li

6 - 7IPN 074-471-P1BHAPSITE ER Operating ManualFigure 6-6 Additional Calibration PointsAdditional compounds are added by following the same steps.

6 - 8 IPN 074-471-P1B HAPSITE ER Operating ManualCAUTIONAll unknown samples should first be collected with the Survey Method to avoid saturating the

7 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 7Tune7.1 Introduction to AutoTune and Manual TuneEnsuring the Mass Spectrometer (MS) perform

7 - 2 IPN 074-471-P1B HAPSITE ER Operating Manual7.2 AutoTuneThere are two versions of the AutoTune program: Short and Long. The Short AutoTune prog

7 - 3IPN 074-471-P1BHAPSITE ER Operating Manual7.2.1 Starting AutoTune from the Manual Tune Screen on the Laptop Computer1 Double-click on the ER I

TOC - 9IPN 074-471-P1BHAPSITE ER Operating Manual11.7 Full Scan Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

7 - 4 IPN 074-471-P1B HAPSITE ER Operating Manual7.3 Viewing a Tune ReportThe Tune Report can be viewed from the front panel display or from the Lap

7 - 5IPN 074-471-P1BHAPSITE ER Operating ManualTo view the Tune Report from the front panel display, touch the HAPSITE icon and then touch TUNE STAT

7 - 6 IPN 074-471-P1B HAPSITE ER Operating Manual7.4 AutoTune FailureOccasionally, AutoTune may fail. Follow the procedures outlined below before co

7 - 7IPN 074-471-P1BHAPSITE ER Operating Manual4 Select default.tun file and press OK. See Figure 7-10.Figure 7-10 Select "default.tun" F

7 - 8 IPN 074-471-P1B HAPSITE ER Operating Manual6 Highlight default.tun. Click OK. See Figure 7-12.NOTE: This will overwrite the default.tun file. I

7 - 9IPN 074-471-P1BHAPSITE ER Operating Manual7.5 Manual Tune Settings and ControlsManual Tune is run from the Laptop computer. The Manual Tune sc

7 - 10 IPN 074-471-P1B HAPSITE ER Operating Manual7.5.1 Tool BarFigure 7-14 Manual Tune Tool BarFilament On/Off . . . . . . . . . Turns the Emissi

7 - 11IPN 074-471-P1BHAPSITE ER Operating ManualShow Bounds . . . . . . . . . . . Displays the peak centroid and the target peak width at 10% peak h

7 - 12 IPN 074-471-P1B HAPSITE ER Operating ManualShow Tune Status Panel . . . . . . . . Displays the Tune and Mass Calibration Status panel.Show Mas

7 - 13IPN 074-471-P1BHAPSITE ER Operating ManualShow Target . . . . . . . . . . . . . . . . . . Displays the target bar for the mass peak center an

TOC - 10 IPN 074-471-P1B HAPSITE ER Operating Manual13.1.3 HSS Indicators . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

7 - 14 IPN 074-471-P1B HAPSITE ER Operating Manual7.5.3 Tune Control PanelFigure 7-17 Tune Control PanelThe Tune Control Panel provides access to d

7 - 15IPN 074-471-P1BHAPSITE ER Operating Manual7.5.3.1 Tune ParametersEM Volt. . . . . . . . . . . . . . . . . . . . . . . Used to increase or dec

7 - 16 IPN 074-471-P1B HAPSITE ER Operating ManualShort AutoTune . . . . . . . . . . . . . . . Starts the Short AutoTune functionLong AutoTune . . .

7 - 17IPN 074-471-P1BHAPSITE ER Operating Manual7.5.4.1 Peak Scan Window ControlsMass Adjust . . . . . . . . . . . . Enables the cursor to select

7 - 18 IPN 074-471-P1B HAPSITE ER Operating Manual7.5.5 Full Scan WindowThe Full scan window (see Figure 7-19) is used for display purposes to evalu

7 - 19IPN 074-471-P1BHAPSITE ER Operating ManualFigure 7-20 Setting the Full Scan RangeDefault Scan ranges of 45 - 300 AMU or 1 - 45 AMU can be sel

7 - 20 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 7-22 Tune and Mass Calibration Status MenuMass . . . . . . . . . . . . . . . . . . . . . .

7 - 21IPN 074-471-P1BHAPSITE ER Operating ManualMax OK Target Percentage . . . . . . Displays the maximum percentage required for the mass peak to m

7 - 22 IPN 074-471-P1B HAPSITE ER Operating ManualDiff(mmu) . . . . . . . . . . . . . . . . . . . . Provides an adjustment to DAC value for mass pea

7 - 23IPN 074-471-P1BHAPSITE ER Operating Manual7.5.8 Right Mouse Button (RMB) MenusIn addition to the functions described above, the following men

TOC - 11IPN 074-471-P1BHAPSITE ER Operating Manual14.8.3 Method Events . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

7 - 24 IPN 074-471-P1B HAPSITE ER Operating Manual7.5.8.2 RMB in Tune Status WindowPlacing the Mouse Cursor in the Tune Status panel or the Mass Cal

7 - 25IPN 074-471-P1BHAPSITE ER Operating Manual7.6 Performing Manual TuneCAUTIONManual Tune is a procedure that should only be attempted by experi

7 - 26 IPN 074-471-P1B HAPSITE ER Operating Manual3 Select default.tun file and press OK. See Figure 7-29.Figure 7-29 Select default.tun File4 Wait

7 - 27IPN 074-471-P1BHAPSITE ER Operating ManualFigure 7-30 Checking BPG and EM VoltageFigure 7-31 BPG Low

7 - 28 IPN 074-471-P1B HAPSITE ER Operating Manual5a If yes, then the BPG does not need adjustment. Proceed to Step 8.5b If no, the BPG will need to

7 - 29IPN 074-471-P1BHAPSITE ER Operating Manual7.6.2 Adjusting Resolution1 Before adjusting Resolution, Base Peak Gain must be adjusted. Refer to

7 - 30 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 7-34 Target Percentage Low3b If the red box is in the Max Target Percentage, the Target Res

7 - 31IPN 074-471-P1BHAPSITE ER Operating Manual2a If the Actual Percentage is above the acceptable range, (red box appears to the right of the colu

7 - 32 IPN 074-471-P1B HAPSITE ER Operating Manual3 After making Ion Energy adjustments:3a If the red boxes no longer appear, indicating the Actual R

7 - 33IPN 074-471-P1BHAPSITE ER Operating ManualFigure 7-38 Tune Saved5 Exit Manual Tune by closing the Tune window. The HAPSITE is ready for sampl

TOC - 12 IPN 074-471-P1B HAPSITE ER Operating Manual15.7.2 Attaching the HAPSITE to the Service Module using the HAPSITE Front Panel Controls . . .

7 - 34 IPN 074-471-P1B HAPSITE ER Operating ManualThis page is intentionally blank.

8 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 8ER IQ Software8.1 The HAPSITE Software - ER IQER IQ™ software includes all of the functions

8 - 2 IPN 074-471-P1B HAPSITE ER Operating Manual8.2 Computer System RequirementsThe following is the minimum recommended laptop computer system for

8 - 3IPN 074-471-P1BHAPSITE ER Operating Manual8.4 Reloading Default HAPSITE MethodsAll of the default methods are saved on the Laptop. These metho

8 - 4 IPN 074-471-P1B HAPSITE ER Operating ManualER_Air_Tri-Bed_PPM_Standard . . Carbon Concentrator Method to be used in lieu of ER_Air_Loop_PPM_Sta

8 - 5IPN 074-471-P1BHAPSITE ER Operating Manual8.4.2 Loading a Default Method to the HAPSITE1 From the Default Methods Menu, select the default met

8 - 6 IPN 074-471-P1B HAPSITE ER Operating Manual4 Double-click the Analyze folder for Analyze methods (or Survey folder for a Survey method). See Fi

8 - 7IPN 074-471-P1BHAPSITE ER Operating Manual5 Double-click on the appropriate folder for the method to be saved. See Figure 8-6.NOTE: If using a

8 - 8 IPN 074-471-P1B HAPSITE ER Operating Manual8.5 Establishing Communications between the HAPSITE and Laptop Computer Establishing communications

8 - 9IPN 074-471-P1BHAPSITE ER Operating ManualFigure 8-9 Add HAPSITE4 The newly added HAPSITE will appear in the HAPSITE List. Press OK. 5 Press O

TOC - 13IPN 074-471-P1BHAPSITE ER Operating Manual16.11 Battery Charger Maintenance and Troubleshooting. . . . . . . . . . . . . . . . . 16-4416.11.

8 - 10 IPN 074-471-P1B HAPSITE ER Operating Manual8.5.2 Configuring the HAPSITE for Communications1 If communication between the HAPSITE and the Lap

8 - 11IPN 074-471-P1BHAPSITE ER Operating ManualFigure 8-13 Network Connections Standard View5 The Network Connection Status Window will open. Clic

8 - 12 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 8-14 Local Area Connection Status Window6 In the General tab, scroll down and highlight Int

8 - 13IPN 074-471-P1BHAPSITE ER Operating Manual7 Select Use the following IP address and enter the IP address of the HAPSITE, (refer to Step 3 on p

8 - 14 IPN 074-471-P1B HAPSITE ER Operating Manual8.5.3 Establishing Communication with the Service ModuleService Module communications will be esta

8 - 15IPN 074-471-P1BHAPSITE ER Operating ManualWhen Add Port is selected, the window shown in Figure 8-20 will appear. Select the appropriate COM p

8 - 16 IPN 074-471-P1B HAPSITE ER Operating Manual8.6 Establishing Communications between the HAPSITE and Laptop Computer Using the Wireless Connect

8 - 17IPN 074-471-P1BHAPSITE ER Operating Manual4 Select the correct Time Zone from the drop-down list above the map.5 Press OK and reboot the HAPSI

8 - 18 IPN 074-471-P1B HAPSITE ER Operating Manual8.8.1 Changing Access LevelsNOTE: When Normal access level is selected, a message will appear stat

8 - 19IPN 074-471-P1BHAPSITE ER Operating Manual8.8.2 Setting or Changing the Access Level Password1 To change the Advanced level password, first e

TOC - 14 IPN 074-471-P1B HAPSITE ER Operating ManualAppendix CShipping the HAPSITE and ConsumablesC.1 Introduction. . . . . . . . . . . . . . . . . .

8 - 20 IPN 074-471-P1B HAPSITE ER Operating Manual8.9 ER IQ ControlsThe System Setup Page is the main screen of the ER IQ software. The System Setup

8 - 21IPN 074-471-P1BHAPSITE ER Operating Manual8.9.1.1 FileThe File drop down menu is shown in Figure 8-32.Figure 8-32 File Menu Selection8.9.1.2

8 - 22 IPN 074-471-P1B HAPSITE ER Operating Manual8.9.1.5 View MenuThe View menu provides selections for displaying and removing parts of the user i

8 - 23IPN 074-471-P1BHAPSITE ER Operating ManualClick on the ER IQ Information icon to check the software version for the Laptop.Figure 8-35 ER IQ

8 - 24 IPN 074-471-P1B HAPSITE ER Operating ManualAccesses methods to initiate a run.Accesses the NIST software and library.Accesses the NIOSH Databa

8 - 25IPN 074-471-P1BHAPSITE ER Operating ManualAccesses Data File information.Returns the current screen to the System Setup screen.Accesses ER IQ

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9 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 9Data Review9.1 Introduction to Data Review The Data Review section of the ER IQ Laptop soft

9 - 2 IPN 074-471-P1B HAPSITE ER Operating Manual9.2 Accessing the Data Review FeatureThe Data Review feature can be accessed as follows: Double-cl

9 - 3IPN 074-471-P1BHAPSITE ER Operating ManualThe Recall window will appear. Select the desired Data File, either from the Laptop or the HAPSITE. S

1 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 1Introduction1.1 The HAPSITE ER SystemThe HAPSITE® ER Portable Gas Chromatograph and Mass Sp

9 - 4 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 9-4 Sections of the Data Review ScreenTIC/RIC Window . . . . . . . . . . . . . . . This wind

9 - 5IPN 074-471-P1BHAPSITE ER Operating Manual9.3 Data Review ToolbarThe Data Review toolbar is shown in Figure 9-5.Figure 9-5 Data Review Toolba

9 - 6 IPN 074-471-P1B HAPSITE ER Operating Manual . . . . . . . . . . . . . . . . . . . . . . . . . Opens AMDIS Program.. . . . . . . . . . . . . . .

9 - 7IPN 074-471-P1BHAPSITE ER Operating ManualFigure 9-7 RMB Menu in TIC/RIC WindowCommon Scale . . . . . . . . . . . . . . . . When checked, all

9 - 8 IPN 074-471-P1B HAPSITE ER Operating ManualPeaks gives you the following submenu:Switch to AMDIS. . . . . . . . . . . . Switches to the AMDIS p

9 - 9IPN 074-471-P1BHAPSITE ER Operating Manual9.4.2 RMB in the Spectrum Display WindowWARNINGBe careful not to subtract data/peaks that may be nee

9 - 10 IPN 074-471-P1B HAPSITE ER Operating ManualUnlock Normalization Cursor . . . . Must be unlocked to move the normalization cursor to a mass oth

9 - 11IPN 074-471-P1BHAPSITE ER Operating Manual9.5 The TIC/RIC Display FunctionsThere are tools available to assist in the Data Review process.9.5

9 - 12 IPN 074-471-P1B HAPSITE ER Operating Manual9.5.2 How to Use Background Subtraction WARNINGBe careful not to subtract a data/peaks that may be

9 - 13IPN 074-471-P1BHAPSITE ER Operating ManualFigure 9-11 Using Background Subtract3 Select the background subtract blue triangle from the lower

OPERATING MANUALIPN 074-471-P1BHAPSITE® ERChemical Identification Systemwww.inficon.com [email protected] ©2008 INFICON

1 - 2 IPN 074-471-P1B HAPSITE ER Operating Manual1.2 Performance SpecificationsThe performance specifications for the HAPSITE are shown below:Mass r

9 - 14 IPN 074-471-P1B HAPSITE ER Operating Manual9.5.2.2 Background Subtraction Using a Range of PointsFigure 9-12 Using Background Subtraction to

9 - 15IPN 074-471-P1BHAPSITE ER Operating Manual9.5.2.3 Additional Features of the Background ToolIf the cursor is placed over B1 or B2, and the Ri

9 - 16 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 9-14 Using the Range Tool9.5.3.1 Steps Required to Range Acquisition1 Place cursor on the

9 - 17IPN 074-471-P1BHAPSITE ER Operating ManualRemove . . . . . . . . . . . . . . . . . . . . . . Removes the Range cursorSelect Mass for Integrati

9 - 18 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 9-16 Selecting Area to Zoom2 Click and hold the LMB at the point in the TIC where Zoom shou

9 - 19IPN 074-471-P1BHAPSITE ER Operating Manual9.6.2 Using The Zoom Spectrum FunctionZooming into a Spectrum requires selection of the Zoom button

9 - 20 IPN 074-471-P1B HAPSITE ER Operating Manual9.7 Displaying Reconstructed Ion Chromatograms (RIC)RIC plots are useful when locating specific co

9 - 21IPN 074-471-P1BHAPSITE ER Operating Manual9.7.1 RIC Plot to Locate Specific CompoundsNOTE: Before running NIST, position the scan cursor over

9 - 22 IPN 074-471-P1B HAPSITE ER Operating Manual7 Enter the three largest peaks in the boxes under the Mass (it may also be shown as Ma...) in the

9 - 23IPN 074-471-P1BHAPSITE ER Operating ManualFigure 9-27 RIC Plot to Locate Benzene — Three Masses Selected11 The compound was not detected in t

1 - 3IPN 074-471-P1BHAPSITE ER Operating Manual1.4 Theory of OperationThe HAPSITE combines two analytical techniques, gas chromatography and mass s

9 - 24 IPN 074-471-P1B HAPSITE ER Operating Manual2 The Spectrum will be displayed in the Spectrum window.3 Press the F7 key, or use the RMB to displ

9 - 25IPN 074-471-P1BHAPSITE ER Operating ManualFigure 9-30 Comparison of NIST and SpectrumIf the Description box is checked, the NIST header infor

9 - 26 IPN 074-471-P1B HAPSITE ER Operating ManualSelect Peaks. The submenu pops up displaying the choices. See Figure 9-31.Figure 9-31 Peaks Menu C

9 - 27IPN 074-471-P1BHAPSITE ER Operating ManualFigure 9-33 Post Analysis DisplayIn Figure 9-33, both the Search for Peaks function and the Label t

9 - 28 IPN 074-471-P1B HAPSITE ER Operating ManualQualitative identification of each peak found by the Search function can be done by checking either

9 - 29IPN 074-471-P1BHAPSITE ER Operating ManualTo print a report of the results, click on the Report Preview button. This will result in the follow

9 - 30 IPN 074-471-P1B HAPSITE ER Operating ManualWhen the analyst invokes AMDIS, upon completion of the analysis, the program returns the Results Sc

9 - 31IPN 074-471-P1BHAPSITE ER Operating ManualFigure 9-38 AMDIS Confirm WindowThis window shows the complete analysis, peak by peak. If there are

9 - 32 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 9-39 NIST Database Search9.8.4 Analyzing Data Using NISTBy right-clicking on the Spectrum

9 - 33IPN 074-471-P1BHAPSITE ER Operating ManualSwitch to NIST Program (F8). . . . . Starts the full NIST program and will place any files that are

1 - 4 IPN 074-471-P1B HAPSITE ER Operating Manual1.5 Instrument OverviewThe HAPSITE system is comprised of two modules: the HAPSITE, also known as

9 - 34 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 9-42 NIST DatabaseNotice the tabs at the bottom of the NIST window. These are multiple wind

9 - 35IPN 074-471-P1BHAPSITE ER Operating ManualFigure 9-43 View Search Results IconFigure 9-44 Search Reports ScreenThere are a maximum of three

9 - 36 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 9-45 Qualitative Report in Excel9.9 ER IQ Hot KeysTable 9-1 ER IQ Hot KeysKeys FunctionsC

9 - 37IPN 074-471-P1BHAPSITE ER Operating ManualCtrl+P PrintPage up Expands the Y Axis view to show twice the current max scale. (If it was 100%, it

9 - 38 IPN 074-471-P1B HAPSITE ER Operating ManualThis page is intentionally blank.

10 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 10Saving and Managing Files10.1 Saving Files on the HAPSITEFile types are created two ways,

10 - 2 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 10-1 Save Method File Dialog Window - HAPSITE Option SelectedEnter the new file name in the

10 - 3IPN 074-471-P1BHAPSITE ER Operating ManualCAUTIONThe HAPSITE ER software is case sensitive. Folder names on the HAPSITE and Laptop must be exa

10 - 4 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 10-4 Method Editor - Showing File Name OptionsThe system allows flexibility to add the Date

10 - 5IPN 074-471-P1BHAPSITE ER Operating ManualNOTE: Tune files are saved, by default, to the HAPSITE hard drive under the Tune folder.Figure 10-5

1 - 5IPN 074-471-P1BHAPSITE ER Operating ManualThe inside of the column is coated with a thin layer of a material known as the stationary phase. The

10 - 6 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 10-7 Save Tune File ScreenOnce the Tune file is saved, the Save Tune File and Manual Tune w

10 - 7IPN 074-471-P1BHAPSITE ER Operating Manual10.1.5 Data ReviewData review is used to view and analyze Data Files. To open files, double-click o

10 - 8 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 10-10 Data Review Recall WindowThe Data File is opened in the Data Review window, as shown

10 - 9IPN 074-471-P1BHAPSITE ER Operating ManualData Files stored on the Laptop may also be opened for review. To open files on the Laptop, select t

10 - 10 IPN 074-471-P1B HAPSITE ER Operating ManualSelecting a different Laptop disk drive is achieved by clicking on the drive drop down box. (Figur

10 - 11IPN 074-471-P1BHAPSITE ER Operating ManualOn the Maintain Logs line of Data Settings, enter either indefinitely or the number of days to save

10 - 12 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 10-15 Manage Files Icon in System Setup ViewThe Manage Files dialog allows the transfer of

10 - 13IPN 074-471-P1BHAPSITE ER Operating ManualFigure 10-17 Manage Files - Rename WindowFiles or folders may be deleted by clicking the file and

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11 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 11Method Editor11.1 The Method EditorCAUTIONOnly trained users should create methods. Selec

1 - 6 IPN 074-471-P1B HAPSITE ER Operating ManualThe performance of the column is affected by temperature, therefore, the column is housed in a tempe

11 - 2 IPN 074-471-P1B HAPSITE ER Operating Manual A Summary page is provided, at the end of the Method Editor, which allows for review and printing

11 - 3IPN 074-471-P1BHAPSITE ER Operating ManualThe order of pages that appear in Wizard mode for various collection and analysis modes are listed i

11 - 4 IPN 074-471-P1B HAPSITE ER Operating Manual11.2 Accessing Method EditorCAUTIONRead all of Chapter 11 before creating a method.To access Metho

11 - 5IPN 074-471-P1BHAPSITE ER Operating ManualFigure 11-6 Method Editor Description PageMode of AnalysisAnalyze (GC/MS). . . . . . . . . . . . .

11 - 6 IPN 074-471-P1B HAPSITE ER Operating ManualCollection ModeFull Scan . . . . . . . . . . . . . . . . . . . . . This mode scans all the masses a

11 - 7IPN 074-471-P1BHAPSITE ER Operating Manual11.3.1 Full Scan MethodA full scan Analyze (GC/MS) method is used for the full identification and q

11 - 8 IPN 074-471-P1B HAPSITE ER Operating Manual11.3.2 SIM MethodThe SIM Analyze (GC/MS) method is used for the identification and quantitation of

11 - 9IPN 074-471-P1BHAPSITE ER Operating Manual11.4 Startup PageCAUTIONTemperature settings are critical to get the proper results. Only trained u

11 - 10 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 11-8 Method Editor Startup Page for Survey MethodsThe parameters on the Startup page are:U

11 - 11IPN 074-471-P1BHAPSITE ER Operating ManualProbe . . . . . . . . . . . . . . . . . . . . . . . . The target temperature the Probe must achieve

1 - 7IPN 074-471-P1BHAPSITE ER Operating Manualmolecules are fractured into smaller molecules, some of which are also ionized. The remaining stream

11 - 12 IPN 074-471-P1B HAPSITE ER Operating Manual11.4.1 HeadspaceCAUTIONOnly trained users should create methods. Choosing the incorrect sampling

11 - 13IPN 074-471-P1BHAPSITE ER Operating Manual11.4.2 SituProbeCAUTIONOnly trained users should create methods. Choosing the incorrect sampling d

11 - 14 IPN 074-471-P1B HAPSITE ER Operating Manual11.5 Inlet PageCAUTIONOnly trained users should modify methods. Changing parameters may result in

11 - 15IPN 074-471-P1BHAPSITE ER Operating ManualFigure 11-12 Method Editor Inlet Page for GC/MS Full ScanOn the Inlet page, the only difference be

11 - 16 IPN 074-471-P1B HAPSITE ER Operating Manual11.5.1 Inlet StatesCAUTIONOnly trained users should modify methods. Changing inlet states may res

11 - 17IPN 074-471-P1BHAPSITE ER Operating ManualHINT: When editing from the keyboard, the Alt+Down Arrow key combination will "drop down"

11 - 18 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 11-15 Valve States for an Inlet State Event

11 - 19IPN 074-471-P1BHAPSITE ER Operating ManualFigure 11-16 Customizing the Valve States for an Inlet StateInlet States can be selected from the

11 - 20 IPN 074-471-P1B HAPSITE ER Operating ManualThe following choices are available in the Inlet States column:Loopfill . . . . . . . . . . . . .

11 - 21IPN 074-471-P1BHAPSITE ER Operating ManualOther . . . . . . . . . . . . . . . . . . . . . . . . This allows the customization of each specifi

1 - 8 IPN 074-471-P1B HAPSITE ER Operating Manual1.6.3 Vacuum SystemThe mass spectrometer is operated in a vacuum for several reasons.  The ions mu

11 - 22 IPN 074-471-P1B HAPSITE ER Operating ManualHSConcDry . . . . . . . . . . . . . . . . . . . This Inlet State allows dry N2 gas to flow through

11 - 23IPN 074-471-P1BHAPSITE ER Operating Manual11.5.2 GC Temperature ProfileCAUTIONOnly trained users should modify methods. Changing GC temperat

11 - 24 IPN 074-471-P1B HAPSITE ER Operating Manual11.5.4 Scan EventsCAUTIONOnly trained users should modify methods. Changing parameters may result

11 - 25IPN 074-471-P1BHAPSITE ER Operating Manual11.5.5 Concentrator SelectionThere are three selections available for the Concentrator:None . . .

11 - 26 IPN 074-471-P1B HAPSITE ER Operating Manual11.6 Tune PageThe Tune Page is divided into two pages, Report and Param, that each provide inform

11 - 27IPN 074-471-P1BHAPSITE ER Operating ManualFigure 11-22 Method Editor Tune Parameter Page - Show Details

11 - 28 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 11-23 Method Editor Tune Report Page

11 - 29IPN 074-471-P1BHAPSITE ER Operating Manual11.7 Full Scan PageCAUTIONOnly trained users should modify methods. Changing parameters may result

11 - 30 IPN 074-471-P1B HAPSITE ER Operating ManualThe following Mass Spectrometer parameters can be programmed:Start Mass . . . . . . . . . . . . .

11 - 31IPN 074-471-P1BHAPSITE ER Operating Manual11.8 SIM PageCAUTIONOnly trained users should modify methods. Changing parameters may result in in

1 - 9IPN 074-471-P1BHAPSITE ER Operating Manual1.6.4 Electronic SystemsThe electronic systems in the HAPSITE are considered in four groups: Mass S

11 - 32 IPN 074-471-P1B HAPSITE ER Operating ManualSIM for the Analyze (GC/MS) mode allows for creation of multiple sets of masses. Each set has a Be

11 - 33IPN 074-471-P1BHAPSITE ER Operating ManualDwell . . . . . . . . . . . . . . . . . . . . . . . . This is the amount of time the Mass Spectrom

11 - 34 IPN 074-471-P1B HAPSITE ER Operating Manual11.8.2 SIM for SurveyFigure 11-26 SIM Page, Differences for Survey Analysis

11 - 35IPN 074-471-P1BHAPSITE ER Operating ManualThe SIM page for Survey mode provides the ability to create only one Scan Set of multiple masses. R

11 - 36 IPN 074-471-P1B HAPSITE ER Operating Manual11.9 Search PageCAUTIONOnly trained users should modify methods. Depending on the search mode sel

11 - 37IPN 074-471-P1BHAPSITE ER Operating ManualThere are four choices in the Search Mode drop down menu.No Search . . . . . . . . . . . . . . . .

11 - 38 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 11-28 AMDIS Search SettingsFigure 11-29 lists the different analysis types available for t

11 - 39IPN 074-471-P1BHAPSITE ER Operating Manualof Retention Index standards. In addition to mass spectral data, if the identified compound is not

11 - 40 IPN 074-471-P1B HAPSITE ER Operating ManualSensitivity . . . . . . . . . . . . . . . . . . . 1-30, used in model peak perception ranges: 30

11 - 41IPN 074-471-P1BHAPSITE ER Operating ManualFigure 11-33 Library OptionsAdvanced SettingsFigure 11-34 Advanced SettingsNOTE: INFICON recommen

1 - 10 IPN 074-471-P1B HAPSITE ER Operating Manual1.6.5 Software SystemsThe HAPSITE operates with two separate software systems. The instrument itse

11 - 42 IPN 074-471-P1B HAPSITE ER Operating ManualReject Bin . . . . . . . . . . . . . . . . . . . . Rejects peaks with less than a set number of sc

11 - 43IPN 074-471-P1BHAPSITE ER Operating ManualWriting a quantitative method still begins with Method Editor, but certain buttons will not be avai

11 - 44 IPN 074-471-P1B HAPSITE ER Operating ManualPeak Resolution (dx) . . . . . . . . . . . This number indicates the minimum number of scans betwe

11 - 45IPN 074-471-P1BHAPSITE ER Operating ManualThe Reset button allows for default values to be reset in the Peak Search window. See Figure 11-38.

11 - 46 IPN 074-471-P1B HAPSITE ER Operating ManualAMDIS . . . . . . . . . . . . . . . . . . . . . . . When enabled, a concentration can be entered.

11 - 47IPN 074-471-P1BHAPSITE ER Operating Manual11.10 Data PageThe Data Page provides the capability to customize the data filenames and storage o

11 - 48 IPN 074-471-P1B HAPSITE ER Operating ManualFile increment digits . . . . . . . . . . . This parameter sets the number of digits used in the

11 - 49IPN 074-471-P1BHAPSITE ER Operating ManualData File Path . . . . . . . . . . . . . . . . . The entry box for the Data File path is used to sp

11 - 50 IPN 074-471-P1B HAPSITE ER Operating Manual11.11 Summary PageThe Summary Page, see Figure 11-45, provides selections to show any component,

11 - 51IPN 074-471-P1BHAPSITE ER Operating Manual11.12 How to Create a MethodCAUTIONOnly trained users should create Methods. Selecting a parameter

2 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 2HAPSITE Components and Assemblies2.1 Ship Kit Packing Lists2.1.1 930-850-G9, G12 Ship Kit

11 - 52 IPN 074-471-P1B HAPSITE ER Operating Manual3 Choose the Method file to be the template for the new Method. Click OK. See Figure 11-48.Figure

11 - 53IPN 074-471-P1BHAPSITE ER Operating ManualFigure 11-49 Save Method File Dialog Window - HAPSITE Option Selected6 On the File Name line, type

11 - 54 IPN 074-471-P1B HAPSITE ER Operating Manual7a If creating a new folder, name the new folder and then open the new folder before saving the Me

11 - 55IPN 074-471-P1BHAPSITE ER Operating Manual3 Type a new name for the sequenced Method or use the name provided. See Figure 11-54.NOTE: Method

11 - 56 IPN 074-471-P1B HAPSITE ER Operating Manual5 Choose a Method file to add to the sequence. Click OK. See Figure 11-55.Figure 11-55 Choose Met

11 - 57IPN 074-471-P1BHAPSITE ER Operating Manual7 In the Start column, choose either Run Button or Immediately for each method. This selection dete

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12 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 12Target Compound Methods12.1 Introduction To Quantitative AnalysisQuantitative analysis is

12 - 2 IPN 074-471-P1B HAPSITE ER Operating Manual12.2 Definition of Terms in the Calibrate WindowFigure 12-1 Calibrate Window12.2.1 MethodBrowse

12 - 3IPN 074-471-P1BHAPSITE ER Operating ManualDisplay. . . . . . . . . . . . . . . . . . . . . . . Displays the chromatogram for the selected Data

TrademarksThe trademarks of the products mentioned in this manual are held by the companies that produce them.ConFlat® is a registered trademark of Va

2 - 2 IPN 074-471-P1B HAPSITE ER Operating ManualBox 2 Contents . . . . 930-470-G1 Battery Charger . . . . 24 V Power Supply (see table)Power sup

12 - 4 IPN 074-471-P1B HAPSITE ER Operating Manual12.2.4 AnalytesAnalytes in Library. . . . . . . . . . . . . Displays the analytes in the libraryAn

12 - 5IPN 074-471-P1BHAPSITE ER Operating ManualArea . . . . . . . . . . . . . . . . . . . . . . . . . Displays the integrated analyte area quant io

12 - 6 IPN 074-471-P1B HAPSITE ER Operating Manual12.3 Definition of Terms in the ID Unknowns WindowFigure 12-4 ID Unknowns Window12.3.1 MethodBro

12 - 7IPN 074-471-P1BHAPSITE ER Operating Manual12.3.3 Peak SearchSearch . . . . . . . . . . . . . . . . . . . . . . . Performs a peak detection an

12 - 8 IPN 074-471-P1B HAPSITE ER Operating ManualCompound . . . . . . . . . . . . . . . . . . . Shows the compound name found in AMDIS, NIST librar

12 - 9IPN 074-471-P1BHAPSITE ER Operating Manual12.4 Display FunctionThe Display button in the Data Files section of both Calibrate and ID Unknowns

12 - 10 IPN 074-471-P1B HAPSITE ER Operating Manualbe added, place the cursor in the mass spectrum window and click the Right Mouse Button to open up

12 - 11IPN 074-471-P1BHAPSITE ER Operating Manual2 After the standard(s) have been prepared, a Method must be developed to collect the data. The met

12 - 12 IPN 074-471-P1B HAPSITE ER Operating Manual3 After the data has been collected, open the Calibration function which can be accessed by clicki

12 - 13IPN 074-471-P1BHAPSITE ER Operating ManualFigure 12-11 Selecting the Type of Quantitative Method3b Click OK.3c The Method File window will b

2 - 3IPN 074-471-P1BHAPSITE ER Operating Manual2.1.2 930-850-G10, G11 Ship Kit ContentsThe following items are provided in a typical 930-850-G6, G7

12 - 14 IPN 074-471-P1B HAPSITE ER Operating Manualfilled in with the detected peaks. The compounds identified by AMDIS will have Compound names and

12 - 15IPN 074-471-P1BHAPSITE ER Operating ManualSelect the Right Mouse Button. The options available are:Duplicate Row. . . . . . . . . . . . . . C

12 - 16 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 12-15 Finished Analytes Chart 10d To finish the template, the concentration of each analyt

12 - 17IPN 074-471-P1BHAPSITE ER Operating ManualFigure 12-17 Save Library Button12 The template is complete and the library is ready for Calibrati

12 - 18 IPN 074-471-P1B HAPSITE ER Operating Manual12d Additional calibration points can be added to the curve at any time by using the Browse button

12 - 19IPN 074-471-P1BHAPSITE ER Operating Manual1a Selecting ID Unknowns will display the Select File Type dialog box used to select the type of qu

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13 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 13Headspace Sampling System13.1 IntroductionThe Headspace Sampling System (HSS) is an acces

13 - 2 IPN 074-471-P1B HAPSITE ER Operating Manual13.1.1 How the HSS OperatesThe function of the HSS is to provide consistent partition of analytes

13 - 3IPN 074-471-P1BHAPSITE ER Operating Manualand moisture from the previous run. During the Purge cycle, the three-way valves change state, assur

2 - 4 IPN 074-471-P1B HAPSITE ER Operating ManualBox 2 Contents . . . . 930-470-G1 Battery Charger . . . . 24 V Power Supply (see table)Power Sup

13 - 4 IPN 074-471-P1B HAPSITE ER Operating Manual13.1.4 Consumables RequiredThe following consumables are required for routine analysis when using

13 - 5IPN 074-471-P1BHAPSITE ER Operating ManualNOTE: Calibration Mixes may be purchased from a variety of laboratory supply businesses in liquid fo

13 - 6 IPN 074-471-P1B HAPSITE ER Operating Manual13.2 Using the HAPSITE with HSSThe following instructions can be used as a guideline for sample an

13 - 7IPN 074-471-P1BHAPSITE ER Operating Manual13.2.2 Loading the VialsWARNINGWear appropriate Personal Protection Equipment (PPE) as advised by t

13 - 8 IPN 074-471-P1B HAPSITE ER Operating Manual5 Adjust the amount of sample in the sample syringe to 20 mL while removing the air bubble. See Fig

13 - 9IPN 074-471-P1BHAPSITE ER Operating Manual6a Rinse the 10 L syringe, with cemented needle (pictured in Figure 13-6), to be used for the injec

13 - 10 IPN 074-471-P1B HAPSITE ER Operating ManualThe following is a set of examples for amounts of standard mix (at 200 and 2000 g/mL) to be injec

13 - 11IPN 074-471-P1BHAPSITE ER Operating Manual13.2.3 Loading the WellsThis section describes the procedure for loading a sample into the well of

13 - 12 IPN 074-471-P1B HAPSITE ER Operating Manual4 Lower the needle, either into an empty well or an empty vial. See Figure 13-8. NOTE: Do not punc

13 - 13IPN 074-471-P1BHAPSITE ER Operating Manual13.2.5 Making the MeasurementTo make a measurement using the HSS, a method is required. To quantif

2 - 5IPN 074-471-P1BHAPSITE ER Operating Manual2.1.3 Ship Kits Box 3 and 4Figure 2-1 USA 24V Power Supply (AC To DC Power Converter) - Box 3and Ba

13 - 14 IPN 074-471-P1B HAPSITE ER Operating Manual13.3.2.1 Flush ProcedureContamination may be flushed from the HSS by disconnecting the Transfer L

13 - 15IPN 074-471-P1BHAPSITE ER Operating Manual13.3.3 Cleaning the HSS WellsThe heating block is constructed of aluminum and is normally easy to

13 - 16 IPN 074-471-P1B HAPSITE ER Operating Manual13.3.4 Decontaminating the HSSThe HSS is designed to be water resistant, but not waterproof. The

13 - 17IPN 074-471-P1BHAPSITE ER Operating Manual13.3.5 Replacing The HSS BatteryReplacement of the battery is performed on an as needed basis. The

13 - 18 IPN 074-471-P1B HAPSITE ER Operating Manual13.3.6 Replacing The HSS Nitrogen CanisterReplacement of the Nitrogen Canister is on an as needed

13 - 19IPN 074-471-P1BHAPSITE ER Operating Manual13.5 Charging the HAPSITE Battery using the HSSHAPSITE batteries may be charged one at a time usin

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14 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 14SituProbe14.1 SituProbe The SituProbe™ Purge and Trap System is a sampling accessory for

14 - 2 IPN 074-471-P1B HAPSITE ER Operating ManualEach compound will partition according to its solubility in the water phase and its vapor pressure.

14 - 3IPN 074-471-P1BHAPSITE ER Operating Manual14.4 Operating SpecificationsEnvironmental Temperature . . . . . . . Operating: 5 to 45 °C, 0-95% R

2 - 6 IPN 074-471-P1B HAPSITE ER Operating Manual2.2.1 Attaching the ProbeTo attach the probe line, plug the LEMO® communication line into the port

14 - 4 IPN 074-471-P1B HAPSITE ER Operating Manual14.5 Consumables 14.5.1 Compressed NitrogenA source of pressurized, ultra high purity Nitrogen is

14 - 5IPN 074-471-P1BHAPSITE ER Operating Manual14.6 Heated ZonesThere are several heated zones that must be maintained when operating the SituProb

14 - 6 IPN 074-471-P1B HAPSITE ER Operating Manual14.7 Valves and SequencesThe SituProbe follows a fixed sequence of events to volatilize, transfer,

14 - 7IPN 074-471-P1BHAPSITE ER Operating Manuala Concentrator is installed, the HAPSITE’s sampling pathway initially bypasses the Concentrator and

14 - 8 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 14-3 Method Editor Screen for a Default Open Loop MethodFigure 14-4 Purge Tube14.8.3 Meth

14 - 9IPN 074-471-P1BHAPSITE ER Operating Manual14.9 Background Cleanup14.9.1 IntroductionThe SituProbe / HAPSITE system, with Concentrator instal

14 - 10 IPN 074-471-P1B HAPSITE ER Operating ManualHAPSITE . . . . . . . . . . . . . . . . . . . . . A simple troubleshooting step will determine if

14 - 11IPN 074-471-P1BHAPSITE ER Operating Manual14.10 Operating Tips14.10.1 Reducing BackgroundOperator judgment is the first and best means of r

14 - 12 IPN 074-471-P1B HAPSITE ER Operating ManualConcentrator exits the analytical column and crosses the membrane into the Mass Spectrometer, the

14 - 13IPN 074-471-P1BHAPSITE ER Operating ManualNOTE: The water standard and sample temperatures should be closely matched for similar purging char

2 - 7IPN 074-471-P1BHAPSITE ER Operating Manual2.2.2 Installing the Gas CanistersCAUTIONOnly open the front panel in a dry, uncontaminated area.The

14 - 14 IPN 074-471-P1B HAPSITE ER Operating Manual14.11.3 CalculationsThe following equation can be used to calculate the volume of standard mix th

14 - 15IPN 074-471-P1BHAPSITE ER Operating Manual14.13 MaintenancePeriodic cleaning is the only maintenance required for the SituProbe accessory. T

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15 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 15Service Module15.1 IntroductionThe Service Module (also called the SM) provides several s

15 - 2 IPN 074-471-P1B HAPSITE ER Operating Manual15.2 Service Module Input PowerService Modules are available in either 110/220 V(ac) (IPN 930-202-

15 - 3IPN 074-471-P1BHAPSITE ER Operating Manual15.3 Components of the Service ModuleThe following section describes the components of both Service

15 - 4 IPN 074-471-P1B HAPSITE ER Operating Manual15.3.4 Foreline Vent ValveThe Foreline Vent Valve is located in the middle of the MDP/Turbo Pump.

15 - 5IPN 074-471-P1BHAPSITE ER Operating Manual15.3.8 Power SupplyThe Service Module Power Supply is a 24 V(dc) supply that provides power to the

15 - 6 IPN 074-471-P1B HAPSITE ER Operating Manual15.4 When to Use the Service ModuleThe Service Module (SM) can be used with the HAPSITE Chemical I

15 - 7IPN 074-471-P1BHAPSITE ER Operating Manual15.5 ER IQ Software for the Service ModuleThe ER IQ Laptop software for the Service Module can be a

2 - 8 IPN 074-471-P1B HAPSITE ER Operating Manual2.2.2.1 How to Change or Remove a Gas CanisterPush the lever located on the right of the canister.

15 - 8 IPN 074-471-P1B HAPSITE ER Operating Manual15.5.1 The Service Module Tab in Properties WindowFigure 15-7 Service Module Tab in Properties Wi

15 - 9IPN 074-471-P1BHAPSITE ER Operating ManualConfigure . . . . . . . . . . . . . . . . . . . . Allows for times and speeds of Service Module com

15 - 10 IPN 074-471-P1B HAPSITE ER Operating ManualIon Pump Status . . . . . . . . . . . . . . . Displays the Ion Pump usage hours. See Figure 15-10.

15 - 11IPN 074-471-P1BHAPSITE ER Operating ManualThe following status items are reported in the Service Module Tab Properties Window. Refer to Figur

15 - 12 IPN 074-471-P1B HAPSITE ER Operating ManualNOTE: If the HAPSITE is already powered on, it does not need to be turned off before placing it on

15 - 13IPN 074-471-P1BHAPSITE ER Operating Manual15.7.1 Attaching the HAPSITE to the Service Module using the ER IQ SoftwareBe sure to connect the

15 - 14 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 15-16 Attach Confirmation Request5 The Roughing Pump will start first, then the Turbo Pump

15 - 15IPN 074-471-P1BHAPSITE ER Operating ManualFigure 15-19 Stop Prepare Button1a If using the push button keys, highlight STOP PREPARE with the

15 - 16 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 15-21 Service Model Attach Button5 A bar graph displaying the progress of the attach will

15 - 17IPN 074-471-P1BHAPSITE ER Operating Manual15.8.1 Using ER IQ Software to Detach1 Be sure to connect the HAPSITE to the Laptop using a crosso

2 - 9IPN 074-471-P1BHAPSITE ER Operating Manual2.2.3 Install BatteryInsert the battery by sliding it into the rectangular opening to the left of th

15 - 18 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 15-26 Detach In Process5 The HAPSITE Vacuum Interconnect valve will close shortly after se

15 - 19IPN 074-471-P1BHAPSITE ER Operating Manual15.9 Physically Removing the HAPSITE from the Service ModuleThe HAPSITE cannot be physically remov

15 - 20 IPN 074-471-P1B HAPSITE ER Operating Manual15.10 Storing the Service ModuleWhen not attached to the HAPSITE, the Service Module should be st

15 - 21IPN 074-471-P1BHAPSITE ER Operating ManualTo place the Service Module in storage, the aluminum storage plug is placed on the opening where th

15 - 22 IPN 074-471-P1B HAPSITE ER Operating ManualThe prompt shown will appear to confirm pumping down the Service Module. See Figure 15-32.Figure 1

15 - 23IPN 074-471-P1BHAPSITE ER Operating ManualTo complete the Service Module storage procedure, turn off the Service Module power switch at the b

15 - 24 IPN 074-471-P1B HAPSITE ER Operating ManualThis page is intentionally blank.

16 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 16Maintenance16.1 IntroductionThe HAPSITE instrument is designed to require minimal service

16 - 2 IPN 074-471-P1B HAPSITE ER Operating Manual16.2 Safety ConsiderationsWARNINGWhen operating, the NEG pump is hot! Do not bypass the programmed

16 - 3IPN 074-471-P1BHAPSITE ER Operating Manual16.3 HAPSITE Symptom - Cause - Remedy ChartTable 16-1 Diagnosing Problems - HAPSITESymptom Cause R

2 - 10 IPN 074-471-P1B HAPSITE ER Operating Manual2.2.5 Connect Laptop (if desired)The HAPSITE ER has two possible configurations for connecting to

16 - 4 IPN 074-471-P1B HAPSITE ER Operating Manual4c. Make sure that there is a full unexpired internal standard canister in the GC, and make sure th

16 - 5IPN 074-471-P1BHAPSITE ER Operating Manual9d. Check turbo speed in Service Module program, If less then 1480 Hz, Service Module pumps may need

16 - 6 IPN 074-471-P1B HAPSITE ER Operating Manual17. Temperature zone fail to heat. 17a. Open heater, or bad controller card. 17a. Contact Customer

16 - 7IPN 074-471-P1BHAPSITE ER Operating Manual16.4 Required Environment for General MaintenanceThe HAPSITE is designed for use in the field, away

16 - 8 IPN 074-471-P1B HAPSITE ER Operating Manual16.5.1 Contamination of the Mass SpectrometerContamination of the Mass Spectrometer manifold can o

16 - 9IPN 074-471-P1BHAPSITE ER Operating Manual16.5.3 Contamination of the Probe and Probe LineContamination of the Probe and Probe Line can occur

16 - 10 IPN 074-471-P1B HAPSITE ER Operating Manual4 With each end of the probe in a separate hand, move the probe handle up and down until methanol

16 - 11IPN 074-471-P1BHAPSITE ER Operating Manual16.5.4 Decontaminating the Outside of the Analytical Module1 Decontamination cap and plug kit numb

16 - 12 IPN 074-471-P1B HAPSITE ER Operating Manual4 Install the green load lock cover (P/N 930-308-P1). See Figure 16-5.Figure 16-5 Green Load Lock

16 - 13IPN 074-471-P1BHAPSITE ER Operating ManualCAUTIONAll caps must be in place and the front door must be firmly shut before decontaminating the

2 - 11IPN 074-471-P1BHAPSITE ER Operating Manual2.3 Helpful GuidelinesA set of helpful guidelines to keep the HAPSITE safe and operational.DON’T…

16 - 14 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 16-8 Pressure Location on HAPSITEFigure 16-9 MS Pressure on the LaptopA MS Vacuum Pressur

16 - 15IPN 074-471-P1BHAPSITE ER Operating Manual16.6.1 Bakeout ProcedureA bakeout can be performed with or without the use of the Service Module.

16 - 16 IPN 074-471-P1B HAPSITE ER Operating Manual16.6.2 Reactivating the NEG PumpReactivating the NEG Pump requires having the Service Module atta

16 - 17IPN 074-471-P1BHAPSITE ER Operating ManualFigure 16-13 Service Window4 Click the Activate NEG button. 5 At the end of the reactivation, the

16 - 18 IPN 074-471-P1B HAPSITE ER Operating Manual16.7.1 Required Tools and Equipment Service Module Laptop computer New NEG Pump. 1/4” Allen w

16 - 19IPN 074-471-P1BHAPSITE ER Operating Manual16.7.2 Part 1: NEG Pump Removal1 This procedure requires the use of a Service Module. The HAPSITE

16 - 20 IPN 074-471-P1B HAPSITE ER Operating ManualWARNINGThe NEG Pump becomes very hot when in operation. The software-controlled sequence to remove

16 - 21IPN 074-471-P1BHAPSITE ER Operating Manual6 Remove chain clamp.7 Pull the NEG Pump out.NOTE: The aluminum gasket can not be reused. Bend the

16 - 22 IPN 074-471-P1B HAPSITE ER Operating Manual3 Wearing safety glasses and gloves, clean the o-ring on the VI valve with methanol. See Figure 16

16 - 23IPN 074-471-P1BHAPSITE ER Operating Manual5 Replace the VI valve into the bottom of manifold. Hand tighten. See Figure 16-20.Figure 16-20 Re

DECLARATION OF CONFORMITY This is to certify that this equipment, designed and manufactured by: INFICON Inc. Two Technology Place

2 - 12 IPN 074-471-P1B HAPSITE ER Operating Manual2.4 HAPSITE ConfigurationsThere are six basic configurations for the HAPSITE. The first three can

16 - 24 IPN 074-471-P1B HAPSITE ER Operating Manual16.7.4 Part 3: Install the New NEG PumpWARNINGGloves must be worn while performing all of the fol

16 - 25IPN 074-471-P1BHAPSITE ER Operating Manual2 Remove the new NEG Pump and aluminum gasket from the shipping container. See Figure 16-23.Figure

16 - 26 IPN 074-471-P1B HAPSITE ER Operating Manual4 Remove the new NEG Pump from the protective container. See Figure 16-25.CAUTIONThe NEG Pump is s

16 - 27IPN 074-471-P1BHAPSITE ER Operating Manual7 Save the rubber “O” ring assembly and container to dispose of the old NEG Pump.8 Place the new al

16 - 28 IPN 074-471-P1B HAPSITE ER Operating Manual10 Replace the chain clamp insuring that the nut points to the left. Use the torque wrench and tig

16 - 29IPN 074-471-P1BHAPSITE ER Operating Manual11 Place the old NEG Pump into the protective container with the o-ring assembly and place back in

16 - 30 IPN 074-471-P1B HAPSITE ER Operating Manual16.7.5 Part 4: Leak Check of the Vacuum SystemCAUTIONChecking for leaks is very important. Air le

16 - 31IPN 074-471-P1BHAPSITE ER Operating ManualFigure 16-33 Select "default.tun" File4 Wait for the automated process of opening tune t

16 - 32 IPN 074-471-P1B HAPSITE ER Operating Manual7 Close the Tune Status Panel and the Mass Calibration Status by deselecting each. See Figure 16-3

16 - 33IPN 074-471-P1BHAPSITE ER Operating Manual10 Select Custom. Type in a range of 60 to 90. This will enable the analyst to scan for both the 69

2 - 13IPN 074-471-P1BHAPSITE ER Operating ManualTransfer Line Insulation (INFICON part number 931-405-P1) — This foam sleeve is used as insulation f

16 - 34 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 16-40 Short Tune Icon15 Follow with section 16.7.6, Part 5: Activation of the NEG Pump, on

16 - 35IPN 074-471-P1BHAPSITE ER Operating ManualFigure 16-42 Service Window4 Select Activate NEG. 5 When prompted on the Front Panel, enter the Se

16 - 36 IPN 074-471-P1B HAPSITE ER Operating Manualprocess. If a NEG has greater than 50 hours (approximately 1/2 the expected life) the more economi

16 - 37IPN 074-471-P1BHAPSITE ER Operating ManualFigure 16-43 Vent HAPSITE from ER IQ SoftwareCAUTIONThe NEG Pump becomes very hot when in operatio

16 - 38 IPN 074-471-P1B HAPSITE ER Operating Manual5 To loosen the chain clamp, turn the nut counter-clockwise until loose. See Figure 16-16.Figure 1

16 - 39IPN 074-471-P1BHAPSITE ER Operating ManualCAUTIONMake sure all tools are clean by wiping them with methanol. Wear powder free gloves for the

16 - 40 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 16-47 Extension Tube Slid into the Ion Volume13 Use the flat head screw driver to loosen t

16 - 41IPN 074-471-P1BHAPSITE ER Operating Manual18 Tighten the three securing screws with the screw driver. Tighten them alternately and gently to

16 - 42 IPN 074-471-P1B HAPSITE ER Operating Manual3 Remove the top cover of the needle assembly to expose the needle and the 1/4" connection fi

16 - 43IPN 074-471-P1BHAPSITE ER Operating ManualFigure 16-51 Holding Down the Needle while Tightening the Nuts (So Ferrules Seat Properly)9 Now th

2 - 14 IPN 074-471-P1B HAPSITE ER Operating Manual4 Plug one end of the Y-cable into the HAPSITE 24 V(dc) connector.5 Plug the other end of the Y-cab

16 - 44 IPN 074-471-P1B HAPSITE ER Operating Manual16.11 Battery Charger Maintenance and TroubleshootingWARNING - Risk Of Electric ShockDo not attem

16 - 45IPN 074-471-P1BHAPSITE ER Operating Manual16.11.2.2 If the Red Indicator is FlashingThis indicates that the Battery Charger is unable to com

16 - 46 IPN 074-471-P1B HAPSITE ER Operating ManualThis page is intentionally blank.

17 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 17Customer Support17.1 How To Contact Customer SupportWorldwide support information regardi

17 - 2 IPN 074-471-P1B HAPSITE ER Operating ManualThis page is intentionally blank.

18 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 18Part Numbers18.1 HAPSITE Part NumberTable 18-1 Part Number Product Feature Options HSER9

18 - 2 IPN 074-471-P1B HAPSITE ER Operating Manual18.2 HAPSITE ER Accessories Service Module930-202-G1 . . . . . . . . . . . . . . . . 100/120/230

18 - 3IPN 074-471-P1BHAPSITE ER Operating ManualLine Insulation070-1545 . . . . . . . . . . . . . . . . . . Probe InsulationNIST930-4071-G1 . . .

18 - 4 IPN 074-471-P1B HAPSITE ER Operating ManualCombo Pack Canisters 930-477-P1. . . . . . . . . . . . . . . . . Gas Combo Pack (4 Carrier Gas and

18 - 5IPN 074-471-P1BHAPSITE ER Operating Manual18.5 Service Module Spare Parts 068-0002 . . . . . . . . . . . . . . . . . . . . . Battery Charger

2 - 15IPN 074-471-P1BHAPSITE ER Operating ManualFigure 2-13 Attaching the Transfer Line to the Back of the HSSFigure 2-14 Attaching Transfer Line

18 - 6 IPN 074-471-P1B HAPSITE ER Operating ManualThis page is intentionally blank.

19 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 19Glossary19.1 GlossaryAir peak . . . . . . . . . . . . . . . . . . . . . . A response by t

19 - 2 IPN 074-471-P1B HAPSITE ER Operating ManualCarrier Gas . . . . . . . . . . . . . . . . . . . The pure inorganic gas used to aid the flow of sa

19 - 3IPN 074-471-P1BHAPSITE ER Operating ManualElution time. . . . . . . . . . . . . . . . . . . The time from injection of a specific compound ont

19 - 4 IPN 074-471-P1B HAPSITE ER Operating ManualFull Method . . . . . . . . . . . . . . . . . . . Full method allows the user to specify a range of

19 - 5IPN 074-471-P1BHAPSITE ER Operating ManualInlet State . . . . . . . . . . . . . . . . . . . . This refers to a specification of the state of

19 - 6 IPN 074-471-P1B HAPSITE ER Operating ManualLibrary . . . . . . . . . . . . . . . . . . . . . . . A user compiled list of compounds, which incl

19 - 7IPN 074-471-P1BHAPSITE ER Operating ManualNIST Library . . . . . . . . . . . . . . . . . . NIST stands for National Institute of Standards an

19 - 8 IPN 074-471-P1B HAPSITE ER Operating ManualRecalculate . . . . . . . . . . . . . . . . . . . An option in the Calibration section of the Run M

19 - 9IPN 074-471-P1BHAPSITE ER Operating Manual% RSD . . . . . . . . . . . . . . . . . . . . . . . Percent Relative Standard Deviation. This is a m

2 - 16 IPN 074-471-P1B HAPSITE ER Operating Manual9 If using the HSS in portable mode, a battery will need to be installed. Open the front door of th

19 - 10 IPN 074-471-P1B HAPSITE ER Operating ManualSituProbe . . . . . . . . . . . . . . . . . . . . The SituProbe Purge and Trap System is a sampli

19 - 11IPN 074-471-P1BHAPSITE ER Operating ManualTune . . . . . . . . . . . . . . . . . . . . . . . . . A term (noun or verb) which generally refers

19 - 12 IPN 074-471-P1B HAPSITE ER Operating ManualThis page is intentionally blank.

A - 1IPN 074-471-P1BHAPSITE ER Operating ManualAppendix AHAPSITE Target CompoundsA.1 Compounds In Order Of Elution Name Formula k Quantion I.S. C

A - 2 IPN 074-471-P1B HAPSITE ER Operating ManualThis page is intentionally blank.

B - 1IPN 074-471-P1BHAPSITE ER Operating ManualAppendix BCalibrating Gas MixturesB.1 Acquisition, Preparation, and HandlingCAUTIONFailure to calibr

B - 2 IPN 074-471-P1B HAPSITE ER Operating ManualB.1.1.1 Using Cylinders Charged with Each ConcentrationTo perform a calibration, have the known gas

B - 3IPN 074-471-P1BHAPSITE ER Operating ManualB.1.1.2 Diluting the Gas On SiteThe comments above, concerning hardware, relate as well to the case

B - 4 IPN 074-471-P1B HAPSITE ER Operating ManualB.1.2.1 Free Flow of GasThe free flow of gas from the regulator of a pressure cylinder is reduced t

B - 5IPN 074-471-P1BHAPSITE ER Operating Manualon-off valves on the Tedlar bags (such as on 231 -XX series bags by SKC5, Inc.) should minimize any f

2 - 17IPN 074-471-P1BHAPSITE ER Operating Manual2.6 Service ModuleThe Service Module is used to create a vacuum in the HAPSITE. It cannot be used i

B - 6 IPN 074-471-P1B HAPSITE ER Operating ManualTedlar bags may be cleaned for reuse, or replaced with new bags. To clean a Tedlar bag for use with

C - 1IPN 074-471-P1BHAPSITE ER Operating ManualAppendix CShipping the HAPSITE and ConsumablesC.1 IntroductionThe HAPSITE instrument and its Service

C - 2 IPN 074-471-P1B HAPSITE ER Operating Manualeasiest approach is to contact INFICON and order the required gases to be shipped directly to the si

C - 3IPN 074-471-P1BHAPSITE ER Operating ManualAlthough the airline will carry the box of canisters in the same cargo hold as the baggage, they will

Index - 1IPN 074-471-P1BHAPSITE ER Operating ManualIndexSymbols% RSD 19-9AAC to DC power converter 2-9airleak 16-3, 16-5samples 1-6alignment 19-1AMD

Index - 2 IPN 074-471-P1B HAPSITE ER Operating Manualcurve statistics 12-4Customer SupportCustomer Service 17-1Repair Service 17-1Return Material Aut

Index - 3IPN 074-471-P1BHAPSITE ER Operating ManualHot Swap Cable 2-43HSPurge 11-21HSS 1-1, 2-12, 5-15, 19-4AC to CD Power 2-13battery 2-16battery c

Index - 4 IPN 074-471-P1B HAPSITE ER Operating Manualmethanol 14-12, 16-22method 19-6development 11-3, 12-11sequencing 11-54wizard 11-2Method EditorI

Index - 5IPN 074-471-P1BHAPSITE ER Operating Manualresolution 11-40, 19-8response factor 12-1, 12-4retention time 1-5, 12-1, 19-8reverse search 19-8

2 - 18 IPN 074-471-P1B HAPSITE ER Operating ManualThe Service Module requires a power cable and a RS-232 communications cable to allow communication

Index - 6 IPN 074-471-P1B HAPSITE ER Operating ManualTTargetlibrary 6-4Tedlar bag B-4, B-6temperatureramp 11-23Tenax concentrator 11-25threshold 19-1

2 - 19IPN 074-471-P1BHAPSITE ER Operating Manual1 Attach the RS-232 communications cable to the Service Module, as shown in Figure 2-20. Figure 2-20

2 - 20 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 2-22 System Setup Screen with Service ModuleNOTE: If the Service Module icon does not appea

2 - 21IPN 074-471-P1BHAPSITE ER Operating ManualFigure 2-24 Cleaning the Service Module Rubber O-ring using a Lint-free WipeAfter cleaning the rubb

Immunity: EN 61326:2006 (EMC – Measurement, Control & Laboratory Equipment) Class A: Immunity per Table A.1 ETSI EN 3

2 - 22 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 2-25 Remove the Green Plastic Protective Cover on the Bottom of the HAPSITEFigure 2-26 show

2 - 23IPN 074-471-P1BHAPSITE ER Operating ManualFigure 2-27 Service Module - Showing Latch on Right SideFigure 2-28 shows the HAPSITE attached to t

2 - 24 IPN 074-471-P1B HAPSITE ER Operating Manual2.6.3 Detaching the HAPSITE from the Service ModuleCarefully follow the procedures starting with s

2 - 25IPN 074-471-P1BHAPSITE ER Operating Manual4 Connect the end of the SituProbe Transfer Line to the HAPSITE at the same location where the probe

2 - 26 IPN 074-471-P1B HAPSITE ER Operating Manual6 OPTIONAL: Insert a charged battery into the SituProbe accessory battery slot. The battery is not

2 - 27IPN 074-471-P1BHAPSITE ER Operating Manual12 The SituProbe accessory (IPN 932-220-G1) displays water level conditions in the purge head. Green

2 - 28 IPN 074-471-P1B HAPSITE ER Operating ManualNOTE: The Tenax Concentrator does not have a specific orientation. See Figure 2-38.Figure 2-38 Ten

2 - 29IPN 074-471-P1BHAPSITE ER Operating ManualFigure 2-39 Placing Concentrator in Bottom Elbow4 For the Tribed Concentrator: Carefully lift up on

2 - 30 IPN 074-471-P1B HAPSITE ER Operating Manual5 Keep the Concentrator aligned between the two elbow fittings while gently pressing down on the to

2 - 31IPN 074-471-P1BHAPSITE ER Operating ManualFigure 2-43 Using Wrench8 Place the black Concentrator Cover (see Figure 2-44) over the Concentrato

DECLARATION OF CONFORMITY This is to certify that this equipment, designed and manufactured by: INFICON Inc. Two Technology Place

2 - 32 IPN 074-471-P1B HAPSITE ER Operating ManualNOTE: The Concentrator Cover contains two metal contacts, inspect the contacts, prior to assembly,

2 - 33IPN 074-471-P1BHAPSITE ER Operating Manual2.8 Probe Sampling Options and AttachmentsTo expand the sampling range of the HAPSITE, sample colle

2 - 34 IPN 074-471-P1B HAPSITE ER Operating Manual2.8.2 Attaching a Bag SampleWhen samples are collected to be run later, various sampling bags can

2 - 35IPN 074-471-P1BHAPSITE ER Operating Manual2.8.3 VX / R-33 Conversion TubeThis procedure describes the steps required to prepare the HAPSITE t

2 - 36 IPN 074-471-P1B HAPSITE ER Operating Manual3 Insert either end of the VX-G Conversion Tube into the nut. Make sure the tube is firmly seated i

2 - 37IPN 074-471-P1BHAPSITE ER Operating Manual2.9 BatteriesThe battery provides power to the HAPSITE to allow portability. Under optimum conditio

2 - 38 IPN 074-471-P1B HAPSITE ER Operating Manual2.9.2 Battery ChargerThe auxiliary Battery Charger (part number 930-470-G1—see Figure 2-52) charge

2 - 39IPN 074-471-P1BHAPSITE ER Operating Manual2.9.2.1 Battery Charger ComponentsThe Battery Charger is shipped with a power cord and spare fuses.

2 - 40 IPN 074-471-P1B HAPSITE ER Operating ManualAmber . . . . . . . . . . . . . . . . . . . . . . . The battery is fully charged. The rate of charg

2 - 41IPN 074-471-P1BHAPSITE ER Operating Manual2.10 Portable AccessoriesPortability is an important HAPSITE feature. The following accessories fac

CE Implementation Date: March 31, 2006 Authorized Representative: Duane H. Wright Operations Quality Manager, ISS INFICON Inc.

2 - 42 IPN 074-471-P1B HAPSITE ER Operating Manual2.10.2 HAPSITE BackpackThe backpack is a light weight, high quality hiker’s backpack. It has been

2 - 43IPN 074-471-P1BHAPSITE ER Operating Manual2.10.2.2 Care of the Backpack Avoid exposing the backpack to solvents and other active chemicals.

2 - 44 IPN 074-471-P1B HAPSITE ER Operating ManualWARNING - Risk Of Electric ShockDo not use if the "L" connector is broken. WARNING - Risk

2 - 45IPN 074-471-P1BHAPSITE ER Operating Manual2.11.2 Storing the Hot Swap CableThe Hot Swap Cable and Battery have exposed electrical connections

2 - 46 IPN 074-471-P1B HAPSITE ER Operating ManualThis page is intentionally blank.

3 - 1IPN 074-471-P1BHAPSITE ER Operating ManualChapter 3Operating HAPSITE in Portable Mode3.1 Starting the HAPSITE in Portable ModePortable Mode re

3 - 2 IPN 074-471-P1B HAPSITE ER Operating Manual4 The HAPSITE will begin to prepare various components. These components include heating the HAPSITE

3 - 3IPN 074-471-P1BHAPSITE ER Operating Manual7 The progress of the preparation is shown by a bar graph. If a component is in the process of being

3 - 4 IPN 074-471-P1B HAPSITE ER Operating Manual11 When the HAPSITE is ready to run samples, a green SYSTEM READY, SURVEY READY or ANALYZE READY mes

3 - 5IPN 074-471-P1BHAPSITE ER Operating Manual12 If SURVEY READY is displayed, touch RUN SURVEY or push SURVEY RUN. Figure 3-7 Survey Ready13 If A

DECLARATION OF CONFORMITY This is to certify that this equipment, designed and manufactured by: INFICON Inc. Two Technology Place

3 - 6 IPN 074-471-P1B HAPSITE ER Operating Manual3.1.1 Emergency Mode (EMER MODE)In an emergency, the concentrator cleanout can be bypassed to allow

3 - 7IPN 074-471-P1BHAPSITE ER Operating Manual3 A confirmation message will be displayed. Touch Yes or push OK SEL to continue. See Figure 3-11.Fig

3 - 8 IPN 074-471-P1B HAPSITE ER Operating ManualFigure 3-13 EMER Mode Inactive6 The HAPSITE ER will run a concentrator cleanout and prepare for gen

3 - 9IPN 074-471-P1BHAPSITE ER Operating ManualFigure 3-15 Concentrator Cleanout3 The HAPSITE will run a concentrator cleanout. See Figure 3-16.Fig

3 - 10 IPN 074-471-P1B HAPSITE ER Operating Manual3.1.2.2 Skip Cleanout1 Touch CONC OPTIONS or use the arrow keys to highlight the CONC OPTIONS butt

3 - 11IPN 074-471-P1BHAPSITE ER Operating Manual3.1.3 Concentrator Cleanout FailureIf the concentrator cleanout is successful, the screen will disp

3 - 12 IPN 074-471-P1B HAPSITE ER Operating Manual3.1.4 Quick Reference SOP - Heat-up and TuneCAUTIONDo not open the front panel in a wet or contami

3 - 13IPN 074-471-P1BHAPSITE ER Operating Manual3.2 Selecting a Different Method Using the SELECT METHOD IconIf the default method is not the desir

3 - 14 IPN 074-471-P1B HAPSITE ER Operating Manual3 The SYSTEM IS NOT READY screen will appear. To select a new method, touch SELECT METHOD or using

3 - 15IPN 074-471-P1BHAPSITE ER Operating Manual5 The PREPARING message will again be displayed. See Figure 3-25. Refer to steps 4-9 of Section 3.2,